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Evaluation of Group Iii Cations

 Analysis of Group Iii Cations Composition

EVALUATION OF GROUP III CATIONS

Precipitation of Group III Cations and Separation in Subgroups

Examination of Subgroup A of Group III Cations

Research of Subgroup B of Group 3 Cations (PART 1)

Analysis of Subgroup B of Group III Cations (PART 2)

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Use decantate from group II cations

Precipitate

Decantate

Consider since Group IIIB.

Consider since Group IIIA.

Centrifuge and separate.

Add 10 drops of 1M HCl.

Wash with couple of drops of H2O.

Medications

Decantate

Centrifuge and individual.

Proceed to Group IV Analysis.

NO

YES

Does medicine occur?

Add 1 ml of NH3 and temperature in drinking water bath intended for 5 minutes.

Add one particular ml of 5% thioacetamide and heat in water bath pertaining to 5 a few minutes.

Use Group IIIA medications.

Add you drop of

Dimethylglyoxime.

Eliminate.

Dilute to 1 ml and divide into 3.

Steam solution and add 6M NH3 until a little bit basic to litmus.

Decantate

Centrifuge and separate.

Medications

Discard.

Add 1 drop of 16M HNO3 and heat in water bathroom for your five mins.

Wash with 4 drops of 1M HCl.

Add three or more drops 12M HCl.

Precipitate

Decantate

Centrifuge and separate.

Let are a symbol of 1 min.

Acidify with 6M HOAc and add many KNO2 deposits

Acidify with 1 Meters HCl and add several NH4CNS crystals.

Nice mixture.

Put equal volume of acetone or perhaps ethanol and agitate the mixture afterwards.

Formation of yellow medications indicates presence of Co3+.

Formation of bright reddish colored pink medicine means existence of Ni2+.

Formation of blue colored solution shows presence of Co2+.

Make use of Group IIIB decantate.

Put 1 cubic centimeters of 4M HNO3 and evaporate.

Dissolve residue in 1 milliliters water and place it in a test conduit.

Add 4M NaOH till precipitate forms. Add one more 10 drops of NaOH.

Add 6th drops of 3% H2O2 and warmth in normal water bath for 5 minutes.

Precipitate

Decantate

Centrifuge and separate.

Proceed to Analysis of Group IIIB (Part 2).

Wash with 10 drops of INGESTING WATER and add you drop of 4M NaOH.

Decantate

Centrifuge and separate.

Precipitate

Development of crimson colored option shows existence of Mn2+.

Formation of red shaded solution shows presence of Fe2+.

Put 1 drop of zero. 2M KSCN

Add tiny amount of NaBIO3 and 2 drops of 4M HNO3.

Add 1 ml of 4M HNO3 and 2 drops of 1M NaNO2. Mix and heat in drinking water bath

Decantate

Centrifuge and separate.

Medications

Boil in water shower.

Discard.

Water down to 1 cubic centimeters and separate into three or more.

Add two drops of 0. 2M K4Fe(CN)6.

Creation of Prussian blue medicine means presence of Fe3+.

Use decantate from component 1 .

Put 6M HOAc until acid to litmus and add 2-3 drops extra.

Centrifuge and separate.

Decantate

Precipitate

Split in two parts.

Add 6M HOAc until medications dissolves through adding 2 drops of aluminon.

Add five drops of 5% thioacetamide then high temperature in drinking water bath.

Put 1M HOAc until acidulent and add a couple of drops of 0. 1M Pb(OAc)2.

Add 1M (NH4)2CO3 until simple.

Add 6M HCl till precipitate dissolves and heat.

Formation of yellow medications shows existence of Cr2+.

Formation of red pond indicates existence of Al3+.

Neutralize with 6M NH3, add 10 drops of 1M HCl and add five drops of K4Fe(CN)6.

Development of gray-green precipitate means presence of Zn2+.

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